HRID1527704

反应详情

EQUATION

反应方程式

REACTANTS

反应物

$结构：C/C(=C\C1=C(Br)C(=O)c2ccccc2C1=O)C(=O)O$

HCID25235467

未命名化合物

$结构：CCC/C(=C\c1c(Br)c(OC)c2ccccc2c1OC)C(=O)O$

HCID68770455

未命名化合物

PRODUCTS

生成物

$结构：CCC/C(=C\C1=C(Br)C(=O)c2ccccc2C1=O)C(=O)O$

HCID68773742

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

Compound 39b was prepared from 99f (0.078 g, 0.21 mmol) as described above for 39a to give 0.033 g (0.10 mmol, 46%) of the product as a yellow solid following flash chromatography (3:7 acetone:hexanes 0.5% AcOH) and recrystallization from Et2O/hexanes.

WORKUP

后处理

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