反应详情

83.7 g of MeOH was added to Zn(OAc)2.2H2O (19.88 g) in a beaker to form 0.85 mol/L zinc acetate solution. 12.72 g of concentrated NaOH aqueous solution (49.8 wt %) was diluted with 83.7 g of MeOH followed by mixing with the Zn(OAc)2 solution under vigorous stirring. The reaction temperature of the system was maintained at 62° C. 4 minutes after the NaOH solution was mixed with the Zn(OAc)2 solution, 80 mL of 0.05 mol/L sodium oleate aqueous solution was added to the reaction solution. White precipitate formed almost immediately after the addition of sodium oleate. The reaction solution was aged at 62° C. for 45 minutes.