HCID 178476752, compound → HCID 178476751, compound

Participants

Reaction Steps

99.4 g Zn(OAc)2.2H2O was added to 1012 ml of Methanol (MeOH) in a 3-necked round bottom flask (RBF) to form a Zn(OAc)2 solution. 43.2 g of KOH was dissolved with 1012 ml of MeOH followed by mixing with the Zn(OAc)2 solution under vigorous stirring. The reaction temperature of the system was maintained at 62° C. 30 seconds after the KOH solution was mixed with the Zn(OAc)2 solution, 10 g KH570 (γ-Methacryloxypropyl trimethoxy silane) dissolved in 506 ml methanol was added to the reaction solution. 2 minutes after the mixing of Zn(OAc)2 solution and the KOH solution, 150 ml DI H2O was added to the reaction solution. The reaction solution was aged at 62° C. for 30 minutes.

Provenance & Evidence