HCID 178476752, compound → Zinc Acetate
Reaction equation
[Zn:1](OC(C)=O)[O:2][C:3]([CH3:5])=[O:4].O.O>CO>[C:3]([O-:4])(=[O:2])[CH3:5].[Zn+2:1].[C:3]([O-:4])(=[O:2])[CH3:5]Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
40 g of MeOH was added to Zn(OAc)2.2H2O (4.97 g) to form zinc acetate solution. 2.16 g of KOH was added to 40 ml of MeOH to form a KOH solution. The KOH solution was then mixed with the Zn(OAc)2 solution under vigorous stirring to form the reaction solution. The reaction temperature was maintained at 60° C. 0.4 g maltose was dissolved in 4.9 ml of distilled water, and subsequently diluted with 20 ml methanol. 45 seconds after the KOH solution was mixed with the Zn(OAc)2 solution, the maltose solution was added to the reaction solution. The resulting solution was aged at 60° C. for 45 minutes.
Sources & evidence
- ORD record
- ord-4b26cb73ed2847b8962760bd20f435da
- Source dataset
- uspto-grants-2015_07
- Patent number
- US09090468B2
Reaction notes
Loading…