HCID 178476752, compound → Zinc Acetate

1240 mL of MeOH was added to Zn(OAc)2.2H2O (121.77 g) to form zinc acetate solution. 54.88 g of KOH was added to 1240 ml of MeOH to form a KOH solution. The KOH solution was then mixed with the Zn(OAc)2 solution under vigorous stirring to form the reaction solution. The reaction temperature was maintained at 60° C. 14.7 g ethylene glycol (EG) was dissolved in 120 ml of distilled water, and subsequently diluted with 310 ml methanol. 30 seconds after the KOH solution was mixed with the Zn(OAc)2 solution, the EG solution was added to the reaction solution. The resulting solution was aged at 60° C. for 45 minutes.

ORD record

ord-a77f118713044966ac5ad9d8754affcd

Source dataset

uspto-grants-2015_07

DOI

10.6084/m9.figshare.5104873.v1

Patent number

US09090468B2