HCID 178476752, compound → HCID 178476751, compound
Reaction equation
[Zn:1]([O:6][C:7]([CH3:9])=[O:8])[O:2][C:3]([CH3:5])=[O:4].O.O>CO>[Zn:1]([O:6][C:7]([CH3:9])=[O:8])[O:2][C:3]([CH3:5])=[O:4]Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
99.4 g Zn(OAc)2.2H2O was added to 1011.4 ml of Methanol (MeOH) in a 3-necked round bottom flask (RBF) to form a Zn(OAc)2 solution. 44.4 g of KOH was dissolved with 1011.4 ml of MeOH followed by mixing with the Zn(OAc)2 solution under vigorous stirring. The reaction temperature of the system was maintained at 62° C. 1 minute after the KOH solution was mixed with the Zn(OAc)2 solution, 14 g hexadecyltrimethoxysilane dissolved in 579.7 ml ethanol was added to the reaction solution. 3 minutes after mixing of the Zn(OAc)2 solution and the KOH solution, 100 ml DI H2O was added to the reaction solution. The reaction solution was aged at 62° C. for 40 minutes.
Sources & evidence
- ORD record
- ord-d08b4f99c3524b13af9d7b75c9c4ae64
- Source dataset
- uspto-grants-2015_07
- Patent number
- US09090468B2
Reaction notes
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