反应详情

99.4 g Zn(OAc)2.2H2O was added to 1011.4 ml of Methanol (MeOH) in a 3-necked round bottom flask (RBF) to form a Zn(OAc)2 solution. 44.4 g of KOH was dissolved with 1011.4 ml of MeOH followed by mixing with the Zn(OAc)2 solution under vigorous stirring. The reaction temperature of the system was maintained at 62° C. 1 minute after the KOH solution was mixed with the Zn(OAc)2 solution, 14 g hexadecyltrimethoxysilane dissolved in 579.7 ml ethanol was added to the reaction solution. 3 minutes after mixing of the Zn(OAc)2 solution and the KOH solution, 100 ml DI H2O was added to the reaction solution. The reaction solution was aged at 62° C. for 40 minutes.