HCID 178476752, compound → Zinc Acetate

946 mL of MeOH was added to Zn(OAc)2.2H2O (93.09 g) to form zinc acetate solution. 41.99 g of KOH was added to 350 ml of MeOH to form a KOH solution. The KOH solution was then mixed with the Zn(OAc)2 solution under vigorous stirring to form the reaction solution. The reaction temperature was maintained at 60° C. 4.69 g Tetraethyl orthosilicate (TEOS) was dissolved in 25 ml of distilled water. 30 seconds after the KOH solution was mixed with the Zn(OAc)2 solution, the TEOS solution was added to the reaction solution. 60 seconds after the KOH solution was mixed with the Zn(OAc)2 solution, 40.8 ml distilled water was added to the reaction solution. 16.81 g KH570 was dissolved in 25 ml of distilled water. 15 minutes and 30 seconds after the KOH solution was mixed with the Zn(OAc)2 solution, the KH570 solution was added to the reaction solution. The resulting solution was continued to age at 60° C. for 45 minutes.

ORD record

ord-51914be1ec424fe5af6a1c583219f2d4

Source dataset

uspto-grants-2015_07

DOI

10.6084/m9.figshare.5104873.v1

Patent number

US09090468B2