HuagongsheHuagongshe Chemistry Print Report · For research reference only
Menadione → HCID 67057830, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Menadione | HCID 4055 | — |
| Reactant | (4-Chlorophenyl)acetic acid | HCID 15880 | — |
| Product | HCID 67057830 | HCID 67057830 | 75% |
Reaction Steps
As starting materials for the coupling reaction menadione and 4-chlorophenylacetic acid were used. Synthesis is realized according to the general procedure described in general procedure of example 1. After chromatography on silica gel (cyclohexane:ethyl acetate=3:1, UV), 6.46 g (21.8 mmol, 75% yield) of P_TM30 were isolated as yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09090549B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-bd1575860bef45b495586b2f9c287a33 |
| Source note | uspto-grants-2015_07 |