HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dibromoethane → 2-Chloro-5-(1-methanesulfonylcyclopropyl)pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dibromoethane | HCID 7839 | — |
| Reactant | 2-Chloro-5-((methylsulfonyl)methyl)pyridine | HCID 45791237 | — |
| Product | 2-Chloro-5-(1-methanesulfonylcyclopropyl)pyridine | HCID 86696144 | 52% |
Reaction Steps
The title compound was prepared from 2-chloro-5-methanesulfonylmethyl-pyridine and 1,2-dibromoethane following a procedure analogous to that described in Step 3 for Intermediate 4. Yield: 52% of theory; Mass spectrum (ESI+): m/z=232/234 (Cl) [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09090605B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-1cb6425b08094207ad4f0ba585da47f0 |
| Source note | uspto-grants-2015_07 |