HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dibromobutane → HCID 67997461, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dibromobutane | HCID 8056 | — |
| Reactant | (5-Bromopyridin-2-yl)acetonitrile | HCID 29927881 | — |
| Product | HCID 67997461 | HCID 67997461 | 78% |
Reaction Steps
The title compound was prepared from (5-bromo-pyridin-2-yl)-acetonitrile and 1,4-dibromobutane following a procedure analogous to that described in Step 3 for Intermediate 4. Yield: 78% of theory; Mass spectrum (ESI+): m/z=251/253 (Br) [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09090605B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-402fd64d61be4a29888af70eb471e447 |
| Source note | uspto-grants-2015_07 |