1,5-Dibromopentane → HCID 67997680, compound

HRID 1528599Notes

Reaction equation

HRID 1528599 reaction equation
[Br:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:8][C:9]#[N:10])=[N:6][CH:7]=1.Br[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16]Br>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([C:8]2([C:9]#[N:10])[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12]2)=[N:6][CH:7]=1

Participants

3

Reactant 2

HCID 81001,5-DibromopentaneHCID 29927881(5-Bromopyridin-2-yl)acetonitrile

Product 1

HCID 67997680HCID 67997680, compoundYield 60%

Procedure

The title compound was prepared from (5-bromo-pyridin-2-yl)-acetonitrile and 1,5-dibromopentane following a procedure analogous to that described in Step 3 for Intermediate 4. Yield: 60% of theory; Mass spectrum (ESI+): m/z=265/267 (Br) [M+H]+.

Sources & evidence

ORD record
ord-c26687f833664a678f2b8a90cc2e8049
Source dataset
uspto-grants-2015_07
Patent number
US09090605B2

Reaction notes

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