Cyclamen aldehyde → HCID 66578857, compound

HRID 1528851Notes

Reaction equation

[Br-].[Br:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[O:13][N:12]=[C:11]([CH3:14])[C:10]=2[CH2:15][P+](C2C=CC=CC=2)(C2C=CC=CC=2)C2C=CC=CC=2)=[CH:5][CH:4]=1.[CH:35]([C:38]1[CH:43]=[CH:42][C:41]([CH2:44][CH:45]([CH3:48])[CH:46]=O)=[CH:40][CH:39]=1)([CH3:37])[CH3:36]>>[Br:2][C:3]1[CH:4]=[CH:5][C:6]([C:9]2[O:13][N:12]=[C:11]([CH3:14])[C:10]=2[CH:15]=[CH:46][CH:45]([CH3:48])[CH2:44][C:41]2[CH:40]=[CH:39][C:38]([CH:35]([CH3:37])[CH3:36])=[CH:43][CH:42]=2)=[CH:7][CH:8]=1

Participants

Reactant 2

HCID 517827Cyclamen aldehyde

HCID 86673638HCID 86673638, compound

Product 1

HCID 66578857HCID 66578857, compound

Procedure

Prepared according to the procedure described in Example 110, Step 2, using [5-(4-bromo-phenyl)-3-methyl-isoxazol-4-ylmethyl]-triphenyl-phosphonium bromide and 3-(4-isopropyl-phenyl)-2-methyl-propionaldehyde

Workup

customPrepared

Sources & evidence

ORD record: ord-b4130755380940ce9fffe90a461d9410
Source dataset: uspto-grants-2015_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09090573B2

Reaction notes

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