HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 66578553, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Ethyl 2-(4-bromophenyl)acetate | HCID 7020609 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 66578553 | HCID 66578553 | — |
Reaction Steps
Ethyl 4-bromophenylacetate (3.0 g, 12.3 mmol) and potassium tert-butoxide (1.38 g, 12.3 mmol) were combined in DMF (35 mL). Benzyl bromide (2.1 g, 12.3 mmol) was added and the reaction was stirred at room temperature for 1 hour. Aqueous workup provided the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09090573B2 |
| Source dataset | uspto-grants-2015_07 |
| ORD ID | ord-afca979674b540ab98f9ebfa8fbd3347 |
| Source note | uspto-grants-2015_07 |