3,3-Dimethylbutanal → HCID 66578601, compound
Reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[O:12][N:11]=[C:10]([CH3:13])[C:9]=2[NH2:14])=[CH:4][CH:3]=1.[CH3:15][C:16]([CH3:21])([CH3:20])[CH2:17][CH:18]=O>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([C:8]2[O:12][N:11]=[C:10]([CH3:13])[C:9]=2[NH:14][CH2:18][CH2:17][C:16]([CH3:21])([CH3:20])[CH3:15])=[CH:6][CH:7]=1Participants
3
Procedure
Prepared according to the procedure described in Example 20, Step 1, using 5-(4-bromo-phenyl)-3-methyl-isoxazol-4-ylamine and 3,3-dimethyl-butyraldehyde.
Workup
- customPrepared
Sources & evidence
- ORD record
- ord-1bcf45bdfdd84c80ab62171f5737acf6
- Source dataset
- uspto-grants-2015_07
- Patent number
- US09090573B2
Reaction notes
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