4-(2-Ethoxycarbonylethyl)benzeneboronic acid → HCID 66578979, compound

HRID 1528952Notes

Reaction equation

HRID 1528952 reaction equation
Br[C:2]1[CH:7]=[CH:6][C:5]([C:8]2[O:12][N:11]=[C:10]([CH3:13])[C:9]=2[CH2:14][S:15][CH2:16][CH2:17][C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)=[CH:4][CH:3]=1.[CH2:24]([O:26][C:27]([CH2:29][CH2:30][C:31]1[CH:36]=[CH:35][C:34](B(O)O)=[CH:33][CH:32]=1)=[O:28])[CH3:25]>>[CH2:24]([O:26][C:27](=[O:28])[CH2:29][CH2:30][C:31]1[CH:36]=[CH:35][C:34]([C:2]2[CH:7]=[CH:6][C:5]([C:8]3[O:12][N:11]=[C:10]([CH3:13])[C:9]=3[CH2:14][S:15][CH2:16][CH2:17][C:18]3[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=3)=[CH:4][CH:3]=2)=[CH:33][CH:32]=1)[CH3:25]

Participants

3

Reactant 2

HCID 38517004-(2-Ethoxycarbonylethyl)benzeneboronic acidHCID 665784465-(4-Bromo-phenyl)-3-methyl-4-phenethylsulfanylmethyl-isoxazole

Product 1

HCID 66578979HCID 66578979, compound

Procedure

Prepared according to the procedure described in Example 1, Step 7, using 5-(4-bromo-phenyl)-3-methyl-4-phenethylsulfanylmethyl-isoxazole and [4-(2-ethoxycarbonylethyl)phenyl]boronic acid.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-0b9f2d9923144415b962ee2df48b7403
Source dataset
uspto-grants-2015_07
Patent number
US09090573B2

Reaction notes

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