5-Hexene-2-one → [5-(4-Bromo-phenyl)-3-methyl-isoxazol-4-yl]-(1-methyl-pent-4-enyl)-amine

HRID 1529001Notes

Reaction equation

HRID 1529001 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[O:12][N:11]=[C:10]([CH3:13])[C:9]=2[NH2:14])=[CH:4][CH:3]=1.[CH3:15][C:16](=O)[CH2:17][CH2:18][CH:19]=[CH2:20]>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([C:8]2[O:12][N:11]=[C:10]([CH3:13])[C:9]=2[NH:14][CH:19]([CH3:20])[CH2:18][CH2:17][CH:16]=[CH2:15])=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 79895-Hexene-2-oneHCID 582185375-(4-Bromophenyl)-3-methylisoxazol-4-amine

Product 1

HCID 66578305[5-(4-Bromo-phenyl)-3-methyl-isoxazol-4-yl]-(1-methyl-pent-4-enyl)-amine

Procedure

Prepared according to the procedure described in Example 24, Step 1, using 5-(4-bromo-phenyl)-3-methyl-isoxazol-4-ylamine and hex-5-en-2-one.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-d3953257eeab4c729dfb8aab2f3e8635
Source dataset
uspto-grants-2015_07
Patent number
US09090573B2

Reaction notes

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