2-Phenylethanethiol → HCID 66578771, compound

HRID 1529119Notes

Reaction equation

HRID 1529119 reaction equation
Br[CH2:2][C:3]1[C:4]([C:9]2[CH:14]=[CH:13][C:12]([Br:15])=[CH:11][CH:10]=2)=[N:5][O:6][C:7]=1[CH3:8].[C:16]1([CH2:22][CH2:23][SH:24])[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1>>[Br:15][C:12]1[CH:13]=[CH:14][C:9]([C:4]2[C:3]([CH2:2][S:24][CH2:23][CH2:22][C:16]3[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=3)=[C:7]([CH3:8])[O:6][N:5]=2)=[CH:10][CH:11]=1

Participants

3

Reactant 2

HCID 781262-PhenylethanethiolHCID 66578529HCID 66578529, compound

Product 1

HCID 66578771HCID 66578771, compound

Procedure

Prepared according to the procedure described in Example 34, Step 4, using 4-bromomethyl-3-(4-bromo-phenyl)-5-methyl-isoxazole and 2-phenyl-ethanethiol.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-27e58440d0044983b7e1ee0c6f7c051c
Source dataset
uspto-grants-2015_07
Patent number
US09090573B2

Reaction notes

Loading…