Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 4674743 | HCID 4674743 | — |
| Product | HCID 68211002 | HCID 68211002 | 84% |
Reaction Steps
Dissolving 20 (6.5 g, 22 mmol) in hot alcohol (150 mL) and adding slowly a mixture of 100% hydrazine hydrate (1.6 mL), concentrated aqueous ammonia (1.7 mL) and alcohol (5 mL). The mixture was stirred at 75° C. for 2 h. The reaction mixture was filtered to give 21 (5.68 g, 84% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09090612B2 |
|---|
| Source dataset | uspto-grants-2015_07 |
|---|
| ORD ID | ord-d6d1de640d9a471e863a4d1af219187d |
|---|
| Source note | uspto-grants-2015_07 |
|---|
