Melamine → 1,3,5-Triazinane-2,4,6-triimine--hydrogen chloride (1/1)

HRID 1530359Notes

Reaction equation

HRID 1530359 reaction equation
[N:1]1[C:8]([NH2:9])=[N:7][C:5]([NH2:6])=[N:4][C:2]=1[NH2:3].[ClH:10].NC(N)=O>O>[ClH:10].[N:1]1[C:8]([NH2:9])=[N:7][C:5]([NH2:6])=[N:4][C:2]=1[NH2:3]

Participants

4

Reactant 2

HCID 7955Melamine3×HCID 101721Urea hydrochloride2×

Product 1

HCID 5220661,3,5-Triazinane-2,4,6-triimine--hydrogen chloride (1/1)

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

16 g of melamine powder obtained from DSM (Netherlands) were added to 67 ml of water in a beaker. Following addition of the melamine powder, 18 ml of urea hydrochloric acid (Novoc ACL) was added dropwise to the beaker with stirring until the pH of the solution reached about 1.5. Addition of the urea hydrochloric acid composition solubilized the melamine powder forming a compound of Formula I (melamine hydrochloride).

Workup

  1. additionwas added dropwise to the beaker

Sources & evidence

ORD record
ord-aeb8e47d853949849b8132f774df4997
Source dataset
uspto-grants-2015_07
Patent number
US09091019B2

Reaction notes

Loading…