HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dibromosalicylaldehyde → HCID 178449914, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dibromosalicylaldehyde | HCID 7024 | — |
| Reactant | N-tert-butylhydroxylamine | HCID 98586 | — |
| Product | HCID 178449914 | HCID 178449914 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 13 using 3,5-dibromo-2-hydroxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 68.7% yield as a yellow crystalline solid, m.p. 111.3° C. (Rf=0.54 on a silica gel plate using 7:3 hexanes/EtOAc as an eluant).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06197826B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-5175da832f654f48a85633dbe044f612 |
| Source note | uspto-grants-2001_03 |