HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromosalicylaldehyde → HCID 178449915, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromosalicylaldehyde | HCID 72863 | — |
| Reactant | N-tert-butylhydroxylamine | HCID 98586 | — |
| Product | HCID 178449915 | HCID 178449915 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 1 using 5-bromo-2-hydroxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 68.7% yield as a yellow crystalline solid, m.p. 118.7° C. (Rf=0.65 on a silica gel plate using 1:1 EtOAc/hexanes as an eluant).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06197826B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-de7a2748ebe648fd8b933d3c61c58394 |
| Source note | uspto-grants-2001_03 |