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HRID1531252

反应详情

EQUATION

反应方程式

HRID 1531252 的结构方程式

REACTANTS

反应物

2
结构：O=Cc1cc([N+](=O)[O-])cc([N+](=O)[O-])c1O
HCID75571

Benzaldehyde, 2-hydroxy-3,5-dinitro-

C7H4N2O6

结构：CC(C)(C)NO
HCID98586

N-tert-Butylhydroxylamine

C4H11NO

PRODUCTS

生成物

1
结构：CC(C)(C)[N+]([O-])=Cc1cc([N+](=O)[O-])cc([N+](=O)[O-])c1O
HCID178449924

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according to the procedure described in Example 13 using 3,5-dinitro-2-hydroxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 4.4% yield as a yellow crystalline solid, m.p. 200.3° C. (Rf=0.15 on a silica gel plate using 10:1 EtOAc/MeOH as an eluant).

WORKUP

后处理

  1. customThe title compound was prepared