2-Thiopheneboronic acid → N-(indan-5-yl)-5-nitro-2-thiophen-2-yl-benzamide

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Reaction Steps

N-(Indan-5-yl)-5-nitro-2-(thiophen-2-yl)-benzamide is prepared similarly to the title compound of Example 3 using the title B compound, 2-bromo-N-(indan-5-yl)-5-nitro-benzamide (0.137 g, 0.380 mmol) and 2-thiopheneboronic acid (0.073 9, 0.570 mmol). 1H NMR (DMSO-d6, 300 MHz): δ 10.59 (1H, s), 8.38 (1H, dd), 8.30 (1H, d), 7.81 (1H, d), 7.73 (1H, d), 7.06 (1H, s), 7.46 (1H, d), 7.30 (1H, d), 7.18 (2H, m), 2.83 (4H, q), 2.01 (2H, m).

Provenance & Evidence