HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Iodobenzenesulfonyl chloride → HCID 70114191, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Iodobenzenesulfonyl chloride | HCID 7399 | — |
| Reactant | Tert-butylcarbamate | HCID 21252905 | — |
| Reactant | HCID 70126287 | HCID 70126287 | — |
| Product | HCID 70114191 | HCID 70114191 | — |
Reaction Steps
Methyl 2-(4-iodophenylsulfonyl)-amino-6-morpholinohex-4-ynoate: The starting t-butyl-carbamate 31a (6.10 g, 18.7 mmol) is deprotected and coupled with pipsyl chloride (5.11 g, 16.84 mmol) as described for compound 31b to give the title compound as a pale yellow tar.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06197770B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-a5122949ff5e4173b7fa89a3517b1324 |
| Source note | uspto-grants-2001_03 |