Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1,3-Diiodopropane | HCID 12314 | — |
| Reactant | 3H-Indole, 2,3,3-trimethyl- | HCID 15427 | — |
| Product | HCID 46209693 | HCID 46209693 | — |
Reaction Steps
To a 50 mL round bottom flask is added 2,3,3-trimethylindolenine (14.4 mmol) and 1,3-diiodopropane (72.7 mmol) and the mixture is stirred at 60° C. under an atmosphere of nitrogen for 16 hours. The resulting solid is recrystallized from ethanol to give 1-[3-iodopropyl]-2,3,3-trimethyl-3H-indolium iodide (40) as crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06197956B1 |
|---|
| Source dataset | uspto-grants-2001_03 |
|---|
| ORD ID | ord-a7c0c5fd9b6d4218ba02520c610c25fa |
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| Source note | uspto-grants-2001_03 |
|---|
