Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 1,2,3-Trimethylcyclopentadiene | HCID 138063 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178425477 | HCID 178425477 | — |
Reaction Steps
Sodium hydride (containing mineral oil; the content of sodium hydride: 60%) (0.80 g) and aniline (0.046 g) were added to the solution of trimethylcyclopentadiene (1.08 g) dissolved in tetrahydrofuran (6.12 g), and stirred at 50° C. for 3 hours. Thus, trimethylcyclopentadienylsodium was obtained in the form of a solution in tetrahydrofuran.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06197990B1 |
|---|
| Source dataset | uspto-grants-2001_03 |
|---|
| ORD ID | ord-be34fdff6d8d4ce9a642a171482e678f |
|---|
| Source note | uspto-grants-2001_03 |
|---|
