HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69489035, compound → HCID 9873775, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69489035 | HCID 69489035 | — |
| Catalyst | Zinc bromide | HCID 10421208 | — |
| Product | HCID 9873775 | HCID 9873775 | — |
Reaction Steps
In analogy to the procedure described in example 1(e), the (3R,4R)-3-[1-(3-acetylamino-propyl)-1,2,3,4-tetrahydro-quinolin-7-ylmethoxy]-4-[4-[3-(2-methoxy-benzyloxy)-propoxy]-phenyl]-piperidine-1-carboxylic acid tert-butyl ester was deprotected with zinc bromide to yield the (3R,4R)-N-[3-[7-(4-[4-[3-(2-methoxy-benzyloxy)-propoxy]-phenyl]-piperidin-3-yloxymethyl)-3,4-dihydro-2H-quinolin-1-yl]-propyl]-acetamide as a light yellow oil; MS: 616 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06197959B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-6445aceafcd44bbf9ac9bc52ae2820ae |
| Source note | uspto-grants-2001_03 |