HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloride methanol → HCID 69486443, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloride methanol | HCID 21893726 | — |
| Reactant | HCID 69488943 | HCID 69488943 | — |
| Product | HCID 69486443 | HCID 69486443 | — |
Reaction Steps
In analogy to the procedure described in example 4(b), the (3R,4R)-4-[4-[3-(2-methoxy-benzyloxy)-propoxy]-phenyl]-3-[1-(3-methoxy-propyl)-1,2,3,4-tetrahydro-quinolin-7-ylmethoxy]-piperidine-1-carboxylic acid tert-butyl ester was deprotected with HCl/methanol to yield the (3R,4R)-4-[4-[3-(2-methoxy-benzyloxy)-propoxy]-phenyl]-3-[1-(3-methoxy-propyl)-1,2,3,4-tetrahydro-quinolin-7-ylmethoxy]-piperidine as a yellow oil; MS: 589 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06197959B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-64c07633649d49d684b310a70d5a75a1 |
| Source note | uspto-grants-2001_03 |