Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | tert-Butyldiphenylchlorosilane | HCID 94078 | — |
| Reactant | Methyl beta-D-glucopyranoside | HCID 445238 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 11761839 | HCID 11761839 | 88.3% |
Reaction Steps
To a stirred solution of methyl β-D-glucopyranoside (5 g, 25.7 mmol) in 51 mL of dry DMF was added at room temperature imidazole (5.46 g, 80.2 mmol) followed by tert-butyldiphenyl-silyl chloride (11.3 mL, 43.4 mmol). The solution was heated to 50° C. for 24 hours and the DMF was removed under reduced pressure. The reaction mixture was diluted with 200 mL of ethyl acetate and washed with H2O (1×100 mL), saturated aqueous NaCl (1×100 mL), and dried over magnesium sulfate. Concentration and flash chromatography (silica, 4% methanol in dichloromethane) provided pure target compound (9.82 g, 88%) as a white foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06197963B1 |
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| Source dataset | uspto-grants-2001_03 |
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| ORD ID | ord-5a941a9b92cb467291b376c7d8a14468 |
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| Source note | uspto-grants-2001_03 |
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