N-bromobutanimide → HCID 77230413, compound

HRID 1531927Notes

Reaction equation

HRID 1531927 reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]([CH:10]=[C:11]([CH3:13])[CH:12]=1)[C:5]([O:7][CH2:8][CH3:9])=[O:6].[Br:14]N1C(=O)CCC1=O>>[Br:14][CH2:1][C:2]1[CH:3]=[C:4]([CH:10]=[C:11]([CH3:13])[CH:12]=1)[C:5]([O:7][CH2:8][CH3:9])=[O:6]

Participants

3

Reactant 2

HCID 67184N-bromobutanimideHCID 88834Ethyl 3,5-dimethylbenzoate

Product 1

HCID 77230413HCID 77230413, compound

Procedure

The subtitle compound was prepared from ethyl 3,5-dimethylbenzoate (2 g) and N-bromosuccinimide (2 g) by the method of example 5 step (i). Purification was by chromatography eluting with 5% ethyl acetate in isohexane Yield 1.85 g.

Workup

  1. customPurification
  2. washeluting with 5% ethyl acetate in isohexane Yield 1.85 g

Sources & evidence

ORD record
ord-d916d26fce2248df95e7ccae945b7faf
Source dataset
uspto-grants-2001_03
Patent number
US06200981B1

Reaction notes

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