HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1531941Generated: October 30, 2026
Potassium Carbonate → HCID 131722443, compound
https://huagongshe.com/reaction/1531941
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Bromodiphenylmethane | HCID 236603 | — |
| Reactant | Methyl 3-[(2-ethoxy-2-oxoethyl)amino]-5-(hydroxymethyl)benzoate | HCID 131722444 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 131722443 | HCID 131722443 | — |
Reaction Steps
A mixture of the product from step (iv) (3 g), potassium carbonate (15.48 g) and bromodiphenylmethane (2.77 g) in dimethylformamide (100 ml) was heated at 50° C. for 24 hours. The mixture was partitioned between ethyl acetate and brine. The organic phase was dried (MgSO4) and evaporated. Purified by chromatography eluting with 30% ethyl acetate in isohexane. Yield 0.51 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06200981B1 |
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| Source dataset | uspto-grants-2001_03 |
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| ORD ID | ord-cfb99fa1f422413482295afedb73c35c |
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| Source note | uspto-grants-2001_03 |
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