Methyl Salicylate → HCID 10491482, compound

HRID 1531943Notes

Reaction equation

HRID 1531943 reaction equation
[C:1]([O:10][CH3:11])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[OH:4].[Br:12][CH2:13][CH2:14]Br>>[Br:12][CH2:13][CH2:14][O:4][C:3]1[CH:5]=[CH:6][CH:7]=[CH:8][C:2]=1[C:1]([O:10][CH3:11])=[O:9]

Participants

3

Reactant 2

HCID 4133Methyl SalicylateHCID 78391,2-Dibromoethane

Product 1

HCID 10491482HCID 10491482, compound

Procedure

The subtitle compound was prepared from methyl salicylate (5 g) and 1,2-dibromoethane (30.67 g) by the method of example 21 step (ii). Purified by chromatography eluting with 10% ethyl acetate in isohexane. Yield 4.9 g.

Workup

  1. customPurified by chromatography
  2. washeluting with 10% ethyl acetate in isohexane

Sources & evidence

ORD record
ord-5fed13dcd268491ba2c2162277821d84
Source dataset
uspto-grants-2001_03
Patent number
US06200981B1

Reaction notes

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