HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Trifluoromethyl)benzenesulfonyl chloride → HCID 22993879, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Trifluoromethyl)benzenesulfonyl chloride | HCID 2777399 | — |
| Reactant | HCID 22993850 | HCID 22993850 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 22993879 | HCID 22993879 | — |
Reaction Steps
Using the method of Example 17.4, 4-(3-chloro-5-pyridyloxy)-3-aminobenzotrifluoride (0.4 g) and 4-trifluoromethylbenzenesulfonyl chloride ((0.339 g ) were combined to provide, after trituration with ether, the title sulfonamide (0.198 g) which was obtained as a crystalline solid. mp 169-171° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06200995B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-c155c30a24ff450c9095e3035dfb8ec8 |
| Source note | uspto-grants-2001_03 |