HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → HCID 10823069, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | 3-Ethoxy-4-methylisoxazole-5-carboxamide | HCID 10559060 | — |
| Product | HCID 10823069 | HCID 10823069 | — |
Reaction Steps
A solution of 3-ethoxy-4-methylisoxazole-5-carboxamide (3.5 g, 21 mmol) in N,N-dimethylformamide dimethyl acetal (15 mL) was stirred at 120° C. for 15 min. After being cooled, the title compound was collected as a colourless crystals (4.2 g, 91%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06200999B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-377e3b10436847b1bc16df6a6904d733 |
| Source note | uspto-grants-2001_03 |