HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 10755030, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 10845679 | HCID 10845679 | — |
| Catalyst | Benzoyl Peroxide | HCID 7187 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 10755030 | HCID 10755030 | 97% |
Reaction Steps
Ethyl 3-Ethoxy-4-methylisoxazole-5-carboxylate (18 g, 91 mmol), NBS (17.5 g, 100 mmol), dibenzoyl peroxide (1 g, 4.1 mmol) in tetrachloromethane (500 mL) was boiled under reflux for 16 h. The mixture was cooled, filtered and concentrated in vacuo to afford the crude title compound (24.5 g, 97%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06200999B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-e01f0c340c884ad8bf0ba4c54b52957e |
| Source note | uspto-grants-2001_03 |