HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyloxonium tetrafluoroborate → Ethyl 4-methyl-2-propoxybenzimidate tetrafluoroborate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyloxonium tetrafluoroborate | HCID 2723982 | — |
| Reactant | 4-Methyl-2-propoxybenzamide | HCID 21250756 | — |
| Product | Ethyl 4-methyl-2-propoxybenzimidate tetrafluoroborate | HCID 21250823 | — |
Reaction Steps
reaction of 4-methyl-2-propoxybenzamide (11.96 g) with triethyloxonium tetrafluoroborate yielded crude ethyl 4-methyl-2-propoxybenzimidate tetrafluoroborate which on reaction with a saturated solution of ethanolic ammonia and treatment with hydrochloric acid yielded 4-methyl-2-propoxybenzamidine hydrochloride, (8.74 g), m.p. 228-30° C.;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06200980B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-c7b72f70aebe4fcbbdd758271b650e9e |
| Source note | uspto-grants-2001_03 |