反应详情

4-(4′-Methylphenoxy)phenyl allyl ether (4.00 g, 16.37 mnmol) was taken up in 1,2-dichlorobenzene (50 mL) and refluxed for 20 h. After cooling, the solvent was removed in vacuo and the resulting crude oil was chromatographed on silica gel (15% ethyl acetate/hexane) to afford 4-(4′-methylphenoxy)-2-allylphenol.

1. temperaturerefluxed for 20 h
2. temperatureAfter cooling
3. customthe solvent was removed in vacuo
4. customthe resulting crude oil was chromatographed on silica gel (15% ethyl acetate/hexane)