HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dichloro-3-nitrobenzoic acid → 2,5-Dichloro-3-nitrobenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dichloro-3-nitrobenzoic acid | HCID 6951 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | 2,5-Dichloro-3-nitrobenzoyl chloride | HCID 10106386 | 87.5% |
Reaction Steps
A mixture of 5.0 parts of 2,5-dichloro-3-nitrobenzoic acid and 16.2 parts of thionyl chloride was refluxed for 24 hours under argon. The reaction mixture was evaporated, yielding 4.74 parts (87.5%) of 2,5-dichloro-3-nitrobenzoyl chloride (interm. 66).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06201119B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-7b546e05a10c48ec8a242c2f379bb601 |
| Source note | uspto-grants-2001_03 |