Phenothiazine → HCID 131722452, compound

Participants

Reaction Conditions

Reaction Steps

In a 1-L, three-necked flask, fitted with a condenser, stirrer, and thermometer were placed 263 g (0.5 mole) of C8F17SO2N(C2H5)H, 15 g of triethylamine, 3 g of phenothiazine, 150 g toluene and 90 g (0.9 mole) of ethyl acrylate. The reaction mixture was stirred and heated at reflux (about 97° C.) for 16 hours to yield the known adduct C8F17SO2N(C2H5)C2H4COOC2H5 in 97% yield as shown by H-NMR analysis. The adduct was isolated by stripping off the toluene solvent, triethyl amine and excess ethyl acrylate under water aspirator pressure.

Provenance & Evidence