HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 20622821, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 20622827 | HCID 20622827 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20622821 | HCID 20622821 | — |
Reaction Steps
To a solution of 4-chlorosulfonyl-2-phenylbenzoyl methionine methyl ester from Example 5E in dichloromethane is added aqueous ammonia and the mixture is stirred until the reaction is judged complete by TLC analysis. The organic phase is separated, dried and evaporated and the product is purified by chromatography on silica gel.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06204293B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-d36415f2be1944bc897d88e410007886 |
| Source note | uspto-grants-2001_03 |