Diethyl Ether → HCID 131722458, compound

HRID 1532867Notes

Reaction equation

HRID 1532867 reaction equation
[CH:1]1([CH2:7][CH2:8][CH:9]([OH:14])[CH2:10][CH2:11][CH2:12][CH3:13])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[CH3:15][O:16][C:17](=[O:33])[C:18]1[CH:23]=[CH:22][C:21](CBr)=[CH:20][C:19]=1[C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][C:27]=1[CH3:32].[CH3:34]COCC>>[CH3:15][O:16][C:17](=[O:33])[C:18]1[CH:23]=[CH:22][CH:21]=[C:20]([CH2:34][O:14][CH:9]([CH2:10][CH2:11][CH2:12][CH3:13])[CH2:8][CH2:7][CH:1]2[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]2)[C:19]=1[C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][C:27]=1[CH3:32]

Participants

4

Reactant 3

HCID 3283Diethyl EtherHCID 22014209HCID 22014209, compoundHCID 234362594-Bromomethyl-2-(2-methylphenyl)benzoic acid methyl ester

Product 1

HCID 131722458HCID 131722458, compound

Procedure

The ether was prepared using the method described in Example 1205B starting with the compound from Example 1192A and 4-bromomethyl-2-(2-methylphenyl)benzoic acid methyl ester, prepared as in Example 1132A-D. m/e (ESI) 437 (MH+)

Sources & evidence

ORD record
ord-27821d08c1b54475a198998d6c18aff1
Source dataset
uspto-grants-2001_03
Patent number
US06204293B1

Reaction notes

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