HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Water → Furo[2,3-c]pyridin-5-ylmethanol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Water | HCID 962 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | HCID 22047292 | HCID 22047292 | — |
| Lösungsmittel | 1,4-Dioxane | HCID 31275 | — |
| Produkt | Furo[2,3-c]pyridin-5-ylmethanol | HCID 22047174 | 70,4% |
Reaktionsschritte
Also to yield the desired compound: Furo[2,3-c]pyridin-5-ylmethyl acetate (1.15 g, 6 mmol) was dissolved in 1,4-dioxane (30 ml) and water (10 ml) and treated with 2N sodium hydroxide solution (12 ml) and stirred at RT for 18 h. The mixture was then partitioned between ethyl acetate and water, the organic layer was dried and evaporated to dryness to provide the desired compound (0.63 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07732461B2 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-adde202e72824f69a5298fe6bf9019ec |
| Quellennotiz | uspto-grants-2010_06 |