HCID 10978133, compound → HCID 11139364, compound

HRID 1533478Notes

Reaction equation

HRID 1533478 reaction equation
[OH:1][C:2]1[CH:17]=[C:16]([OH:18])[C:5]2[C:6](=O)[CH2:7][C:8]3[CH:14]=[CH:13][CH:12]=[CH:11][C:9]=3[S:10][C:4]=2[CH:3]=1.COC1C=C(OC)C2C(=O)CC3C=CC=CC=3SC=2C=1>>[C:16]1([OH:18])[C:5]2[CH2:6][CH2:7][C:8]3[CH:14]=[CH:13][CH:12]=[CH:11][C:9]=3[S:10][C:4]=2[CH:3]=[C:2]([OH:1])[CH:17]=1

Participants

3

Reactant 2

HCID 10978133HCID 10978133, compoundHCID 11044360HCID 11044360, compound

Product 1

HCID 11139364HCID 11139364, compound

Procedure

The invention further relates in essence to a process for producing diaryl sulfide derivatives or salts thereof in which 7,9-dihydroxy-10,11-dihydrodibenzo[b,f]thiepin-10-one which is the diol compound of the formula (6) or 7,9-dimethoxy-10,11-dihydrodibenzo[b,f]thiepin-10-one which is the dimethoxy compound of the formula (5) is reduced and deprotected to yield 10,11-dihydrodibenzo[b,f]thiepin-1,3-diol of the formula (7):

Sources & evidence

ORD record
ord-8e9f812899df45f499249e9530ad4cf0
Source dataset
uspto-grants-2001_03
Patent number
US06207837B1

Reaction notes

Loading…