Trifluoroacetic acid → HCID 70194114, compound

Participants

Reaction Steps

A solution containing 5.0 g (6.08 mmol) of N,N,N′,N″,N″-pentakis[(tert-butoxycarbonyl)methyl]-2-[(4-nitrophenyl)methyl]-6-methyldiethylenetriamine in 35 ml of trifluoroacetic acid was allowed to stir at room temperature for 48 h. The solvent was removed under reduced pressure and the resultant solid dried under vacuum to produce 4.02 g of product as a pale yellow solid with a yield of 74.75%.

Provenance & Evidence