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HRID1533670

反应详情

EQUATION

反应方程式

HRID 1533670 的结构方程式

REACTANTS

反应物

2
结构：C[C@H](NC(=O)Cc1cc(F)cc(F)c1)C(=O)O
HCID12135350

N-[(3,5-difluorophenyl)acetyl]alanine

C11H11F2NO3

结构：COC(=O)C(N)c1cccs1
HCID13848532

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)C(NC(=O)[C@H](C)NC(=O)Cc1cc(F)cc(F)c1)c1cccs1
HCID22894858

未命名化合物

PROCEDURE

实验过程

Following General Procedure C and using N-(3,5-difluorophenylacetyl)-L-alanine (from Example B2 above) and methyl 2-amino-2-(2-thienyl)acetate (prepared from L-α-2-thienylglycine (Sigma) using General Procedure G), the title compound was prepared as a solid (mp=161-162° C.). The product was purified by preparative LC 2000 chromatography using 1:4 EtOAc/hexanes.

WORKUP

后处理

  1. customThe product was purified by preparative LC 2000 chromatography