HuagongsheHuagongshe Chemistry Print Report · For research reference only
Alanine methyl ester hydrochloride → N-[N-(Phenylacetyl)-L-alaninyl]-L-alanine Methyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Alanine methyl ester hydrochloride | HCID 2733257 | — |
| Reactant | N-(Phenylacetyl)-L-alanine | HCID 7004640 | — |
| Product | N-[N-(Phenylacetyl)-L-alaninyl]-L-alanine Methyl Ester | HCID 22895047 | — |
Reaction Steps
Following General Procedure A and using N-(phenylacetyl)-L-alanine (from Example B1 above) and L-alanine methyl ester hydrochloride (Aldrich), the title compound was prepared as a solid (mp=140.5-142° C.). The reaction was monitored by tlc (Rf=0.17 in 50% EtOAc/hexanes).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06207710B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-e5542be5708c449ab09c4f45978a9fb0 |
| Source note | uspto-grants-2001_03 |