HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl vinyl ether → HCID 54566162, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl vinyl ether | HCID 8023 | — |
| Reactant | Diphenylacetic Acid | HCID 8333 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54566162 | HCID 54566162 | — |
Reaction Steps
Diphenylacetic acid 2-ethoxyethyl ester was prepared in the following manner: To a mixture of 2.0 g (9.4 mmol) of diphenylacetic acid in 10 ml of dichloromethane was added 1.1 ml (0.82 g, 11.4 mmol) of ethyl vinyl ether. The mixture was allowed to stir overnight at which point the reaction mixture was washed with aqueous sodium bicarbonate, dried with MgO-MgSO4, and concentrated in vacuo to give 1.7 g (6.0 mmol, 63% yield) of the corresponding ethoxy ethyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05085972 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-c1510bafa4c14b4f9198995f0c685a29 |
| Source note | uspto-grants-1992_02 |