HRID1533907

反应详情

EQUATION

反应方程式

HRID 1533907 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 1-(4-ethylaminophenyl)-4-phenylmethylpiperazine in ethanol is catalytically hydrogenated at about 70° C. and 50 p.s.i., in the presence of 10% palladium on carbon. After hydrogen uptake ceases, the catalyst is removed by filtration and the filtrate concentrated to obtain the title compound.

WORKUP

后处理

  1. customis catalytically hydrogenated at about 70° C.
  2. customAfter hydrogen uptake ceases, the catalyst is removed by filtration
  3. concentrationthe filtrate concentrated