HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butylamine → HCID 14880464, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butylamine | HCID 6385 | — |
| Reactant | HCID 14880463 | HCID 14880463 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14880464 | HCID 14880464 | — |
Reaction Steps
A solution of 4.65 g of the product of Step A, 100 ml of ethanol and 9.94 ml of tert-butylamine was stirred at reflux for 2 hours and the solution was distilled to dryness. The 6.83 g of residue were chromatographed on silica (eluant: ethyl acetate triethylamine (9-1)) to obtain 4.77 g of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05086070 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-9f7b7086d7f14c3897b22248ce467efc |
| Source note | uspto-grants-1992_02 |