1-Bromo-3-chloropropane → HCID 14880470, compound

Participants

Reaction Steps

Using the procedure of Step E of Example 1, 10.9 g of the product of Step D and 18.17 ml of 1-bromo-3-chloro propane were reacted to obtain after chromatography on silica (eluant: methylene chloride - hexane (75-25)), 14.4 g of the desired product melting at 94° C., which was used as is for the following step.

Provenance & Evidence